Cited Article: Ghosh, S. Carbon nanotube flow sensors
Alert Expires: 09 NOV 2010
Number of Citing Articles: 1 new records this week (1 in this e-mail)
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Title:
Synthesis, Growth Mechanism, and Properties of Open-Hexagonal and Nanoporous-Wall Ceria Nanotubes Fabricated via Alkaline Hydrothermal Route
Authors:
Wu, XS; Kawi, S
Author Full Names:
Wu, Xusheng; Kawi, Sibudjing
Source:
CRYSTAL GROWTH & DESIGN 10 (4): 1833-1841 APR 2010
Language:
English
Document Type:
Article
KeyWords Plus:
MIXED-OXIDE NANOTUBES; BORON-NITRIDE NANOTUBES; CARBON NANOTUBES; CO OXIDATION; ROOM-TEMPERATURE; TITANIA NANOTUBES; NI/Y2O3 CATALYSTS; CO3O4 NANOTUBES; SUPPORTED GOLD; WS2 NANOTUBES
Abstract:
Ce(OH)(3) open-hexagonal nanotubes [Ce(OH)(3)-OH-NT] and Ce(OH)(3) nanoporous-wall nanotubes [Ce(OH)(3)-NW-NT] have been successfully synthesized, for the first time, by a hydrothermal alkaline route and characterized by X-ray diffraction, field emission scanning electron microscopy, transmission electron microscopy, Brunauer-Emmett-Teller method, differential thermal analysis-thermogravimetric analysis, and temperature-programmed reduction, The growth mechanism of Ce(OH)(3)-OH-NT via a hydrothermal alkaline route has been found to occur by the dissolution and recrystallization of surrounding Ce(OH)(3) compounds followed by anisotropical growth of Ce(OH)(3)-OH-NT gradually along the c-axis of nanotubes. The growth of Ce(OH)(3)-OH-NT has been observed, for the first time, to occur over two different Ce(OH)(3) compound bases: multidirectional growth of Ce(OH)(3)-OH-NT over a Ce(OH)(3) spherical core base to obtain nanotube flowers and vertical growth of Ce(OH)(3)-OH-NT over a !
Ce(OH)(3) flat base to obtain a nanotube jungle. Ce(OH)(3)-NW-NT has been successfully fabricated by further treating Ce(OH)(3)-OH-NT under static alkaline treatment at room temperature. Calcination of Ce(OH)(3)-OH-NT and Ce(OH)(3)-NW-NT leads to the formation of CeO2 open-hexagonal nanotubes (CeO2-OH-NT) and CeO2 nanoporous-wall nanotubes (CeO2-NW-NT), respectively. CeO2-OH-NT and CeO2-NW-NT are found to have higher surface area, easier reducibility, and higher mobility of surface oxygen species than CeO2 nanoparticles (CeO2-NP).
Reprint Address:
Kawi, S, Natl Univ Singapore, Dept Chem & Biomol Engn, 4 Engn Dr 4, Singapore 119260, Singapore.
Research Institution addresses:
[Wu, Xusheng; Kawi, Sibudjing] Natl Univ Singapore, Dept Chem & Biomol Engn, Singapore 119260, Singapore
E-mail Address:
chekawis@nus.edu.sg
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Cited Reference Count:
98
Times Cited:
0
Publisher:
AMER CHEMICAL SOC; 1155 16TH ST, NW, WASHINGTON, DC 20036 USA
Subject Category:
Chemistry, Multidisciplinary; Crystallography; Materials Science, Multidisciplinary
ISSN:
1528-7483
DOI:
10.1021/cg901515r
IDS Number:
577OV
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